Si3N4-SiCp composites reinforced by in situ co-catalyzed generated Si3N4 nanofibers
Huang, J; Huang, Z; Zhang, S; et al.Fang, M; Liu, Y
Date: 1 January 2014
Article
Journal
Journal of Nanomaterials
Publisher
Hindawi Publishing Corporation
Publisher DOI
Abstract
Si 3 N 4 - SiC p composites reinforced by in situ catalytic formed nanofibers were prepared at a relatively low sintering temperature. The effects of catalyst Co on the phase compositions, microstructures, and physicochemical-mechanical properties of samples sintered at 1350°C-1450°C were investigated. The results showed that the ...
Si 3 N 4 - SiC p composites reinforced by in situ catalytic formed nanofibers were prepared at a relatively low sintering temperature. The effects of catalyst Co on the phase compositions, microstructures, and physicochemical-mechanical properties of samples sintered at 1350°C-1450°C were investigated. The results showed that the catalyst Co enhanced the nitridation of Si. With the increase of Co addition (from 0 wt% to 2.0 wt.%), the apparent porosity of as-prepared refractories was initially decreased and subsequently increased, while the bulk density and the bending strength exhibited an opposite trend. The Si 3 N 4 - SiC p composites sintered at 1400°C had the highest strength of 60.2 MPa when the Co content was 0.5 wt.%. The catalyst Co facilitated the sintering of Si 3 N 4 - SiC p composites as well as the formation of Si3N4 nanofibers which exhibited network connection and could improve their strength. © 2014 Juntong Huang et al.
Engineering
Faculty of Environment, Science and Economy
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